Synthesis and Application of [2.2]Paracyclophane Derivatives in Catalysis and Material Science

By (author) Christoph Zippel

Book cover: Synthesis and Application of [2.2]Paracyclophane Derivatives in Catalysis and Material Science

Extent: 215, 215 pages

Publisher: Logos Verlag Berlin

Subjects: Earth & Life Sciences 

Series: Beiträge zur organischen Synthese

Series volume number: 96

Language: English

Paperback (Published)

(November 2021)

ISBN: 9783832554125

5.71 x 8.27 inches

Price: $68.00

Out of stock

[2.2]Paracyclophane is a prevalent p-stacked, carbocyclic scaffold with a “bent and battered” structure. This results not only in a transannular communication but also in a chiral plane within the molecule if at least one substituent is present. These unique properties make this structure synthetically challenging but also scarcely investigated. A new method for enantio-separation based on kinetic resolution was developed, which allows the access to enantiomerically pure [2.2]paracyclophane-based building blocks. In a liquid crystal templated chemical vapor deposition process, [2.2]paracyclophanyl alcohols containing an additional central chiral element were evaluated for the self-assembly of nanofibers. Furthermore, the cyclopropanation of a-alkyl-a-diazo compounds with a [2.2]paracyclophane-based rhodium tetracarboxylate complex was investigated. Finally, the rigidity, regioselective functionalization, and transannular communication of [2.2]paracyclophane were exploited in the design of heterobimetallic Au(I)/Ru(II) complexes for the study of metal-to-metal interactions.

  • By (author) Christoph Zippel

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