Structure-activity correlations and solid-state kinetic investigations of iron oxide-based catalysts supported on SBA-15

By (author) Nina Sharmen Genz

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Extent: 257, 257 pages

Publisher: Logos Verlag Berlin

Subjects: Earth & Life Sciences 

Language: English

Paperback (Published)

(October 2019)

ISBN: 9783832549244

5.71 x 8.27 inches

Price: $66.00

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In this book, iron oxidic species supported on nanostructured silica (SBA-15) are introduced as model catalysts for deducing structure-activity correlations in selective oxidation of propene. Influence of iron loading, Fe(III) precursor, powder layer thickness during calcination, and molybdenum addition on structure and activity of FexOy/SBA-15 catalysts is investigated. FexOy/SBA-15 catalysts are characterized ex situ and in situ by a multitude of analyzing methods, i.e. XRD, DR-UV-Vis spectroscopy, N2 physisorption, Raman and Mossbauer spectroscopy, GC-MS, X-ray absorption spectroscopy, and TPR. Moreover, applicability of solid-state kinetic analysis methods to supported iron oxidic species is shown. Results from solid-state kinetic analysis under non-isothermal conditions are particularly helpful in corroborating structure-activity correlations of FexOy/SBA-15 catalysts. Understanding the correlation of various synthesis parameters with structure and activity of FexOy/SBA-15 catalysts eventually permits obtaining improved green iron oxide catalysts for selective oxidation of propene.

  • By (author) Nina Sharmen Genz

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